8GPX
YFV_E_YD73Fab_postfusion
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-07-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 3 2 1 |
Unit cell lengths | 102.874, 102.874, 178.663 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.930 - 3.800 |
R-factor | 0.2635 |
Rwork | 0.261 |
R-free | 0.30590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5jhl |
RMSD bond length | 0.002 |
RMSD bond angle | 0.540 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.19_4092) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 3.940 |
High resolution limit [Å] | 3.800 | 3.800 |
Rmerge | 0.188 | 0.866 |
Number of reflections | 11224 | 1088 |
<I/σ(I)> | 8.082 | |
Completeness [%] | 99.4 | |
Redundancy | 3.6 | |
CC(1/2) | 0.627 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 289.15 | 0.2 M imidazole malate, pH 5.5, and 33% (v/v) PEG 600 |