8GOY
SulE P44R
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-09-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.353, 139.450, 58.125 |
Unit cell angles | 90.00, 101.67, 90.00 |
Refinement procedure
Resolution | 47.310 - 1.784 |
Rwork | 0.159 |
R-free | 0.18530 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4q34 |
RMSD bond length | 0.007 |
RMSD bond angle | 0.918 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (v1.16) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.310 | 1.820 |
High resolution limit [Å] | 1.780 | 1.780 |
Number of reflections | 74840 | 3200 |
<I/σ(I)> | 11.7 | |
Completeness [%] | 98.3 | |
Redundancy | 6.3 | |
CC(1/2) | 0.997 | 0.572 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | PEG 4000 |