8GN4
The crystal structure of ZBTB10 ZF1-2 R767Q in complex with telomeric DNA TTAGGG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 1 |
Unit cell lengths | 30.866, 32.665, 36.105 |
Unit cell angles | 105.99, 90.46, 105.21 |
Refinement procedure
Resolution | 30.188 - 1.900 |
R-factor | 0.2125 |
Rwork | 0.210 |
R-free | 0.25910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8gn3 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.19) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 40.000 | 40.000 | 1.930 |
High resolution limit [Å] | 1.900 | 5.150 | 1.900 |
Rmerge | 0.039 | 0.023 | 0.300 |
Rmeas | 0.046 | 0.027 | 0.362 |
Rpim | 0.024 | 0.014 | 0.201 |
Total number of observations | 31985 | ||
Number of reflections | 9392 | 473 | 356 |
<I/σ(I)> | 9 | ||
Completeness [%] | 91.7 | 93.8 | 71.5 |
Redundancy | 3.4 | 3.7 | 2.7 |
CC(1/2) | 0.998 | 0.905 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Sodium Cacodylate, pH 6.5, 27 % v/v PEG 2000 MME |