8GL7
AncAR1 - progesterone - Tif2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 173 |
Detector technology | PIXEL |
Collection date | 2023-02-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 69.714, 69.714, 144.439 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.300 - 2.400 |
R-factor | 0.1999 |
Rwork | 0.197 |
R-free | 0.25270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 0.992 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.20_4459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.300 | 2.486 |
High resolution limit [Å] | 2.372 | 2.400 |
Rmeas | 0.423 | |
Rpim | 0.088 | 0.411 |
Number of reflections | 14581 | 4584 |
<I/σ(I)> | 1.77 | |
Completeness [%] | 97.0 | 91 |
Redundancy | 22.5 | |
CC(1/2) | 0.990 | 0.726 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% PEG 4000, 0.1M Tris pH 8.9, 4% glycerol |