8GH5
Implementing Logic Gates in DNA Crystal Engineering
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-B |
Synchrotron site | APS |
Beamline | 23-ID-B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-11 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0332 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 51.260, 51.238, 105.514 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 36.240 - 2.640 |
R-factor | 0.2295 |
Rwork | 0.226 |
R-free | 0.28440 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8ep8 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.308 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.757 | 3.133 |
High resolution limit [Å] | 2.640 | 2.640 |
Number of reflections | 3246 | 196 |
<I/σ(I)> | 7.4 | 1.3 |
Completeness [%] | 82.8 | |
Redundancy | 5.9 | |
CC(1/2) | 0.996 | 0.810 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | 10 uM of each motif, 5 mM magnesium sulfate hydrate, 5 mM HEPES sodium, 0.16 M lithium sulfate monohydrate, pH 7.0 |