8G53
Crystal structure of a bacterial TPAT family transporter
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-10-30 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97946 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 52.945, 59.029, 62.543 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 33.340 - 1.030 |
Rwork | 0.165 |
R-free | 0.18290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.059 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.340 | 1.067 |
High resolution limit [Å] | 1.030 | 1.030 |
Number of reflections | 91316 | 5924 |
<I/σ(I)> | 26.55 | |
Completeness [%] | 93.7 | |
Redundancy | 8.3 | |
CC(1/2) | 0.999 | 0.784 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2 M Lithium Sulfate 0.1 M Tris: HCl, pH 8.5 1.26 M Ammonium Sulfate |