8G1C
Crystal structure of polyreactive 3B03 human Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-17 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 1 |
Unit cell lengths | 52.420, 66.170, 90.238 |
Unit cell angles | 104.09, 93.31, 91.60 |
Refinement procedure
Resolution | 64.120 - 1.630 |
R-factor | 0.2025 |
Rwork | 0.202 |
R-free | 0.23580 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.863 |
Data reduction software | iMOSFLM |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 64.120 | 1.690 |
High resolution limit [Å] | 1.630 | 1.632 |
Number of reflections | 132793 | 13000 |
<I/σ(I)> | 27.55 | |
Completeness [%] | 88.5 | |
Redundancy | 6.8 | |
CC(1/2) | 0.643 | 0.314 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 298 | 25% PEG4000, 0.2M Ammonium sulfate, 0.1M Sodium acetate pH 4.6 |