8G19
Crystal structure of monoreactive 4C05 human Fab
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-07-17 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 79.839, 70.609, 87.680 |
Unit cell angles | 90.00, 108.95, 90.00 |
Refinement procedure
Resolution | 39.540 - 1.770 |
R-factor | 0.1886 |
Rwork | 0.187 |
R-free | 0.21940 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.017 |
Data reduction software | iMOSFLM |
Data scaling software | pointless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.540 | 1.833 |
High resolution limit [Å] | 1.770 | 1.770 |
Number of reflections | 44160 | 4398 |
<I/σ(I)> | 11.61 | |
Completeness [%] | 98.0 | |
Redundancy | 1.9 | |
CC(1/2) | 0.998 | 0.924 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | 30% PEG 5000 MME, 0.2M Ammonium sulfate, 0.1M MES pH 6.5 |