8FZZ
Phocaeicola vulgatus type VI secretion system Ntox15 effector and immunity Tde2/Tdi2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2020-03-01 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.311, 84.769, 175.940 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.040 - 2.680 |
R-factor | 0.1905 |
Rwork | 0.185 |
R-free | 0.25080 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 0.933 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX (v1.20.1) |
Refinement software | PHENIX (v1.20.1) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.100 | 2.720 |
High resolution limit [Å] | 2.680 | 2.680 |
Rmerge | 0.160 | 1.200 |
Number of reflections | 42063 | 601 |
<I/σ(I)> | 19.6 | 2 |
Completeness [%] | 98.3 | 85.2 |
Redundancy | 13.5 | 10.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 5% PEG 3350 (w/v), 200 mM NaCl, and 100 mM sodium citrate pH 5.0 |