8FWP
Crystal Structure of CDC10 - CDC3 heterocomplex from Saccharomyces cerevisiae
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | LNLS SIRIUS BEAMLINE MANACA |
Synchrotron site | LNLS SIRIUS |
Beamline | MANACA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-09-29 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.97718 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 83.547, 83.547, 220.262 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.030 - 2.220 |
R-factor | 0.192 |
Rwork | 0.190 |
R-free | 0.22570 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.951 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 46.030 | 43.030 | 2.350 |
High resolution limit [Å] | 2.220 | 6.590 | 2.220 |
Rmerge | 0.297 | 0.067 | 3.570 |
Rmeas | 0.303 | 0.069 | 3.637 |
Rpim | 6.800 | 80.200 | |
Number of reflections | 39667 | 1702 | 6248 |
<I/σ(I)> | 11.99 | 1.2 | |
Completeness [%] | 99.9 | ||
Redundancy | 26 | ||
CC(1/2) | 0.996 | 0.996 | 0.448 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 283 | 0.2 M Sodium formate 0.1 M Bis-Tris propane 6.5 20 % w/v PEG 3350 |