8FSK
LSD1-CoREST in complex with T18, short soaking
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-06-22 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.9677 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 119.391, 179.911, 235.331 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 59.700 - 3.130 |
R-factor | 0.1996 |
Rwork | 0.199 |
R-free | 0.22260 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.356 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 106.470 | 3.240 |
High resolution limit [Å] | 3.120 | 3.120 |
Rmerge | 0.158 | 4.539 |
Rmeas | 0.164 | 4.713 |
Rpim | 0.044 | 1.252 |
Total number of observations | 619486 | 58842 |
Number of reflections | 44804 | 4305 |
<I/σ(I)> | 13.9 | 0.6 |
Completeness [%] | 98.5 | |
Redundancy | 13.8 | 13.7 |
CC(1/2) | 0.999 | 0.299 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 1.2 Sodium/Potassium Tartrate, 100 mM ADA pH 6.5 |