8FJ9
Structure of the catalytic domain of Streptococcus mutans GtfB in tetragonal space group P4322
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-06-11 |
Detector | DECTRIS EIGER2 S 16M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 43 2 2 |
Unit cell lengths | 150.130, 150.130, 302.783 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 75.700 - 2.500 |
R-factor | 0.21363 |
Rwork | 0.212 |
R-free | 0.24086 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 1.299 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0257) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.920 | 2.540 |
High resolution limit [Å] | 2.500 | 2.500 |
Rmerge | 0.314 | |
Rmeas | 0.322 | |
Rpim | 0.072 | 0.882 |
Total number of observations | 2410102 | |
Number of reflections | 119867 | 5852 |
<I/σ(I)> | 9.3 | |
Completeness [%] | 100.0 | 99.8 |
Redundancy | 20.1 | 21 |
CC(1/2) | 0.996 | 0.439 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 295 | 2 M ammonium sulfate, 0.1 M Bis-Tris |