8FHA
Intramolecular ester bond-containing repeat domain 1 from Suipraoptans intestinalis adhesin
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-07-07 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95372 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.051, 104.712, 52.587 |
Unit cell angles | 90.00, 91.81, 90.00 |
Refinement procedure
Resolution | 48.027 - 1.490 |
Rwork | 0.166 |
R-free | 0.21210 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.309 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.090 | 1.520 |
High resolution limit [Å] | 1.490 | 1.490 |
Number of reflections | 81829 | 3553 |
<I/σ(I)> | 10.5 | |
Completeness [%] | 96.6 | 84.8 |
Redundancy | 5.9 | 5.4 |
CC(1/2) | 0.999 | 0.350 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M HEPES, 70% MPD |