8FAX
Fab 1249A8-MERS Stem Helix Complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 113 |
Detector technology | PIXEL |
Collection date | 2022-03-22 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 52.714, 56.308, 76.124 |
Unit cell angles | 90.00, 91.19, 90.00 |
Refinement procedure
Resolution | 43.760 - 2.100 |
R-factor | 0.1853 |
Rwork | 0.182 |
R-free | 0.23970 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.903 |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 45.300 | 2.130 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.119 | 0.436 |
Number of reflections | 26255 | 5954 |
<I/σ(I)> | 5 | |
Completeness [%] | 93.9 | |
Redundancy | 3 | |
CC(1/2) | 0.967 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 290 | 0.2 M magnesium chloride, 0.1 M Tris, pH 8.5, 20% PEG8000 |