8EZT
Crystal structure of HipB(Lp) from Legionella pneumophila
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2019-04-29 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 59.444, 33.488, 74.161 |
Unit cell angles | 90.00, 102.73, 90.00 |
Refinement procedure
Resolution | 22.020 - 2.060 |
R-factor | 0.2996 |
Rwork | 0.297 |
R-free | 0.34310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2wiu |
RMSD bond length | 0.004 |
RMSD bond angle | 0.520 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20_4459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 23.000 | 2.100 |
High resolution limit [Å] | 2.060 | 2.060 |
Rmerge | 1.046 | 0.450 |
Rpim | 0.054 | 0.271 |
Number of reflections | 18042 | 888 |
<I/σ(I)> | 15.6 | 2 |
Completeness [%] | 99.8 | |
Redundancy | 3.9 | |
CC(1/2) | 0.911 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2 M ammonium sulfate, 25% PEG 4K, 0.1 M sodium acetate pH 4.6. cryo paratone |