8EE9
Human PU.1 ETS-Domain (165-270) Bound to d(AATAAAAGGAATGGGG)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-02-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 42.873, 61.185, 44.590 |
Unit cell angles | 90.00, 117.16, 90.00 |
Refinement procedure
Resolution | 33.290 - 1.220 |
R-factor | 0.1445 |
Rwork | 0.144 |
R-free | 0.15610 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8e3k |
RMSD bond length | 0.010 |
RMSD bond angle | 1.238 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 33.290 | 1.264 |
High resolution limit [Å] | 1.220 | 1.220 |
Rmerge | 0.040 | 0.385 |
Rmeas | 0.047 | 0.458 |
Rpim | 0.025 | 0.243 |
Number of reflections | 59154 | 5594 |
<I/σ(I)> | 18.56 | 4.18 |
Completeness [%] | 96.9 | 92.4 |
Redundancy | 3.7 | 3.4 |
CC(1/2) | 0.997 | 0.917 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.6 | 293 | 2% PEG 3350, 100 mM Sodium Acetate, pH 4.6 |