8EBF

C-terminal (TPR) domain of LIC11990 from Leptospira interrogans

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I04
Synchrotron site	Diamond
Beamline	I04
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-07-02
Detector	DECTRIS EIGER2 XE 16M
Wavelength(s)	0.97948
Spacegroup name	P 21 21 21
Unit cell lengths	50.656, 100.093, 170.205
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	43.680 - 2.500
R-factor	0.2377
Rwork	0.235
R-free	0.27760
Structure solution method	SAD
RMSD bond length	0.007
RMSD bond angle	0.860
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	CRANK2
Refinement software	BUSTER (2.10.4 (8-JUN-2022))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.680	2.540
High resolution limit [Å]	2.500	2.500
Rmeas	0.090	1.800
Number of reflections	29774	1503
<I/σ(I)>	11.9	1
Completeness [%]	96.5	98.8
Redundancy	6.5	6
CC(1/2)	0.999	0.600

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	9	293	18% (w/v) PEG 3350, 0.3 M magnesium acetate