8DYI
IL17A homodimer bound to Compound 5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2016-02-17 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 1.00 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 172.938, 30.507, 50.239 |
Unit cell angles | 90.00, 102.71, 90.00 |
Refinement procedure
Resolution | 38.830 - 2.280 |
R-factor | 0.274 |
Rwork | 0.272 |
R-free | 0.31140 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4hr9 |
RMSD bond length | 0.008 |
RMSD bond angle | 1.158 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 42.170 | 2.272 |
High resolution limit [Å] | 2.260 | 2.264 |
Number of reflections | 12501 | 102 |
<I/σ(I)> | 8.4 | |
Completeness [%] | 97.9 | |
Redundancy | 3.2 | |
CC(1/2) | 0.990 | 0.802 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 290.15 | 3.2M NaCl, 0.1M Tris, pH 8.5 |