8DMT
Crystal structure of macrodomain CG2909 from Drosophila melanogaster in complex with ADP-ribose
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL12-2 |
Synchrotron site | SSRL |
Beamline | BL12-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-21 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 48.949, 90.006, 212.267 |
Unit cell angles | 90.00, 95.89, 90.00 |
Refinement procedure
Resolution | 38.490 - 2.280 |
R-factor | 0.1967 |
Rwork | 0.196 |
R-free | 0.23590 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | AlphaFold RE54994p |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 38.490 | 2.362 |
High resolution limit [Å] | 2.280 | 2.280 |
Number of reflections | 77326 | 5609 |
<I/σ(I)> | 8.9 | |
Completeness [%] | 92.2 | |
Redundancy | 6.8 | |
CC(1/2) | 0.984 | 0.658 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M ammonium citrate, 12% w/v PEG3350 |