8DMQ
Crystal structure of Legionella pneumophila macrodomain MavL in complex with ubiquitin vinyl methyl ester
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-E |
Synchrotron site | APS |
Beamline | 24-ID-E |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-08-12 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 108.719, 108.719, 209.143 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 69.710 | 2.273 |
High resolution limit [Å] | 2.195 | 2.195 |
Number of reflections | 73681 | 7171 |
<I/σ(I)> | 14.95 | |
Completeness [%] | 99.7 | |
Redundancy | 10.3 | |
CC(1/2) | 0.978 | 0.725 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.2 M sodium citrate, 20% w/v PEG 3350 |