8DKD
Sliding clamp from M. thermoresistibile
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2019-03-06 |
Detector | RDI CMOS_8M |
Wavelength(s) | 1 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 102.408, 102.408, 134.159 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.970 - 3.200 |
R-factor | 0.2593 |
Rwork | 0.257 |
R-free | 0.27710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3p16 |
RMSD bond length | 0.002 |
RMSD bond angle | 0.506 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.790 | 3.200 |
High resolution limit [Å] | 3.200 | 3.200 |
Rmerge | 0.084 | 0.910 |
Rpim | 0.030 | |
Number of reflections | 12983 | 243 |
<I/σ(I)> | 24.8 | |
Completeness [%] | 93.0 | |
Redundancy | 8.2 | |
CC(1/2) | 0.990 | 0.595 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 4 M ammonium acetate , 0.1 M bis-tris propane, 8% glycerol |