8DEZ
Abp2D Receptor Binding Domain ACICU
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CMOS |
Collection date | 2019-09-06 |
Detector | RDI CMOS_8M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 51.176, 51.176, 128.236 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.530 - 1.290 |
R-factor | 0.2022 |
Rwork | 0.202 |
R-free | 0.20570 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3u4k |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.530 | 1.336 |
High resolution limit [Å] | 1.290 | 1.290 |
Rmerge | 0.040 | 0.685 |
Rmeas | 0.056 | 0.970 |
Number of reflections | 41674 | 5543 |
<I/σ(I)> | 15.57 | 0.9 |
Completeness [%] | 95.0 | 65.35 |
Redundancy | 2 | |
CC(1/2) | 0.999 | 0.520 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 292.15 | 0.1 M Li2SO4, 0.1 M Sodium Citrate and 15% Ethanol |