8DDP
Crystal structure of SRS57 from Toxoplasma gondii
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRL BEAMLINE BL9-2 |
Synchrotron site | SSRL |
Beamline | BL9-2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-10-14 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9791 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 48.130, 59.710, 101.420 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.472 - 1.591 |
R-factor | 0.1704 |
Rwork | 0.169 |
R-free | 0.19120 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1kzq |
RMSD bond length | 0.008 |
RMSD bond angle | 1.275 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHENIX |
Refinement software | PHENIX (1.9_1692) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.480 | 1.620 |
High resolution limit [Å] | 1.590 | 1.590 |
Rmerge | 0.064 | 0.490 |
Number of reflections | 40027 | 1927 |
<I/σ(I)> | 12.6 | |
Completeness [%] | 100.0 | |
Redundancy | 5.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 25% PEG1500 |