8D7D
Crystal structure of hen egg white lysozyme at 225 Kelvin (Triplicate)
Experimental procedure
Experimental method | LAUE |
Source type | ROTATING ANODE |
Source details | BRUKER TURBO X-RAY SOURCE |
Temperature [K] | 225 |
Detector technology | CMOS |
Collection date | 2020-11-04 |
Detector | BRUKER PHOTON 100 |
Wavelength(s) | 1.54184 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 79.487, 79.487, 37.495 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 22.498 - 1.500 |
Rwork | 0.171 |
R-free | 0.20710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3a8z |
RMSD bond length | 0.013 |
RMSD bond angle | 1.838 |
Data reduction software | SAINT |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 22.500 | 22.500 |
High resolution limit [Å] | 1.500 | 1.500 |
Number of reflections | 19769 | 18747 |
<I/σ(I)> | 5.87 | |
Completeness [%] | 99.6 | |
Redundancy | 1.89 | |
CC(1/2) | 0.827 | 0.827 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 4.6 | 295 | 1.2 M NaCl and 100 mM AcONa pH 4.6 |