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8CYL

Ast89 P domain

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsESRF BEAMLINE BM30A
Synchrotron siteESRF
BeamlineBM30A
Temperature [K]291.15
Detector technologyPIXEL
Collection date2017-11-10
DetectorDECTRIS PILATUS 6M-F
Wavelength(s)1.00
Spacegroup nameP 21 21 21
Unit cell lengths74.590, 78.410, 100.860
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution42.415 - 1.888
R-factor0.1644
Rwork0.163
R-free0.19490
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)4x1w
RMSD bond length0.004
RMSD bond angle0.770
Data reduction softwareXDS
Data scaling softwareXSCALE
Phasing softwarePHENIX
Refinement softwarePHENIX ((1.13_2998: ???))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]42.42542.425
High resolution limit [Å]1.8881.888
Number of reflections4732047320
<I/σ(I)>9.19
Completeness [%]98.2
Redundancy1.36
CC(1/2)0.9030.903
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP291.150.1 M citric acid (pH 4) and 30% PEG6000

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