8CPP

CRYSTAL STRUCTURES OF CYTOCHROME P450-CAM COMPLEXED WITH CAMPHANE, THIOCAMPHOR, AND ADAMANTANE: FACTORS CONTROLLING P450 SUBSTRATE HYDROXYLATION

Experimental procedure

Spacegroup name	P 21 21 21
Unit cell lengths	108.670, 103.900, 36.380
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	10.000 * - 2.100
R-factor	0.175
RMSD bond length	0.020
RMSD bond angle	0.036 *
Refinement software	PROFFT

Data quality characteristics

	Overall
High resolution limit [Å]	2.090 *
Rmerge	0.058 *
Total number of observations	133336 *

Crystallization Reagents in Literatures

ID	crystal ID	solution	reagent name	concentration (unit)	details
1	1	1	P-450CAM	1 (mM)	camphor free
2	1	1		250 (mM)
3	1	1	dithiothreitol	50 (mM)
4	1	2	ammonium sulfate	66-70 (%sat)	with 5M KOH