8CNL
Lymphocytic choriomeningitis virus 3'-5' exonuclease domain of nucleoprotein
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-03 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.976260 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 95.076, 95.066, 129.130 |
Unit cell angles | 90.00, 97.54, 90.00 |
Refinement procedure
Resolution | 81.150 - 2.800 |
R-factor | 0.2736 |
Rwork | 0.273 |
R-free | 0.27980 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.368 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 94.254 | 94.254 | 4.470 |
High resolution limit [Å] | 2.800 | 4.470 | 3.170 |
Number of reflections | 310351 | 20129 | 36665 |
<I/σ(I)> | 10.2 | 13.4 | 6.35 |
Completeness [%] | 99.9 | ||
Redundancy | 6.5 | ||
CC(1/2) | 0.996 | 0.995 | 0.982 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.8 | 298 | 0.05M Sodium cacodylate pH 6.8, 0.01M Magnesium sulfate, 2M Ammonium sulfate |