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8CJV

Structure of bovine CD46 ectodomain (SCR 1-4)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsDIAMOND BEAMLINE I03
Synchrotron siteDiamond
BeamlineI03
Temperature [K]100
Detector technologyPIXEL
Collection date2019-12-02
DetectorDECTRIS EIGER2 X 16M
Wavelength(s)0.976
Spacegroup nameP 41 21 2
Unit cell lengths129.731, 129.731, 120.193
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution88.170 - 2.840
R-factor0.2543
Rwork0.253
R-free0.28550
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.015
RMSD bond angle1.840
Data reduction softwareautoPROC
Data scaling softwareSTARANISO
Phasing softwarePHASER
Refinement softwarePHENIX (1.18.2_3874)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]91.7303.240
High resolution limit [Å]2.8402.840
Rmerge0.4872.225
Rmeas0.4972.278
Rpim0.0970.473
Number of reflections10884544
<I/σ(I)>7.11.8
Completeness [%]93.3
Redundancy25.620.5
CC(1/2)0.9980.630
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP6.429310.5mg/ml in 0.1M sodium cacodylate tetrahydrate pH 6.4, 14% PEG smear broad, 0.2M CaCl2, 5% glycerol .

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