8CHO
CRYSTAL STRUCTURE OF DELTA5-3-KETOSTEROID ISOMERASE FROM PSEUDOMONAS TESTOSTERONI
Experimental procedure
Spacegroup name | P 65 2 2 |
Unit cell lengths | 61.680, 61.680, 143.600 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 10.000 - 2.300 |
R-factor | 0.205 |
Rwork | 0.205 |
R-free | 0.27100 |
RMSD bond length | 0.012 * |
RMSD bond angle | 1.615 * |
Phasing software | X-PLOR (3.0) |
Refinement software | X-PLOR (3.2) |
Data quality characteristics
Overall | |
High resolution limit [Å] | 2.300 * |
Completeness [%] | 95.0 * |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | Vapor diffusion, hanging drop * | 7.5 * | 12 * |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | reservoir | ammonium sulfate | 1.3 (M) | |
2 | 1 | reservoir | PEG400 | 3-5 (%) | |
3 | 1 | reservoir | HEPES | 0.1 (M) | |
4 | 1 | drop | protein | 5 (mg/ml) |