8CD8
Ulilysin - C269A with AEBSF complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-06-04 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97866 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 50.130, 124.660, 86.900 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 62.330 - 1.650 |
R-factor | 0.2077 |
Rwork | 0.207 |
R-free | 0.24290 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.901 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX (1.18.2_3874) |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 86.900 | 1.650 |
High resolution limit [Å] | 1.650 | 1.650 |
Rmeas | 0.125 | 0.125 |
Number of reflections | 66338 | 66008 |
<I/σ(I)> | 11.8 | |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 100 mM MES pH 6.5, 200 mM calcium chloride, 18% polyethylene glycol 8000 |