8C46
N-Carbamoyl-beta-Alanine Amidohydrolases from Rhizobium radiobacter MDC 8606
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-12-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.91188 |
Spacegroup name | P 2 21 21 |
Unit cell lengths | 53.231, 104.622, 145.372 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 84.917 - 2.000 |
Rwork | 0.229 |
R-free | 0.26980 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.851 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | MoRDa |
Refinement software | BUSTER |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 84.920 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Number of reflections | 55817 | 4087 |
<I/σ(I)> | 7.1 | 1.3 |
Completeness [%] | 100.0 | |
Redundancy | 7 | |
CC(1/2) | 0.996 | 0.786 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | 23 % (w/v) PEG1500 and 100 mM MMT pH 6.0 |