8BZB
co-soak stabilizers for ERa - 14-3-3 interaction (884_AZ275)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SEALED TUBE |
Source details | RIGAKU MICROMAX-003 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2017-06-23 |
Detector | DECTRIS PILATUS 200K |
Wavelength(s) | 1.541870 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 81.905, 112.491, 62.402 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.950 - 1.700 |
R-factor | 0.1649 |
Rwork | 0.163 |
R-free | 0.19330 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.036 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | PHENIX (1.19.2-4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 66.210 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Number of reflections | 31123 | 1174 |
<I/σ(I)> | 28.7 | |
Completeness [%] | 97.0 | |
Redundancy | 5.8 | |
CC(1/2) | 0.999 | 0.967 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 277 | 0.095 M HEPES (pH 7.1), PEG400 (24% (v/v)), 0.19 M CaCl2 and 5% (v/v) Glycerol |