8BLN
Structure of RutB
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-07-18 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 58.115, 125.107, 123.268 |
Unit cell angles | 90.00, 93.22, 90.00 |
Refinement procedure
Resolution | 41.000 - 1.880 |
R-factor | 0.2527 |
Rwork | 0.250 |
R-free | 0.29630 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | WT model |
RMSD bond length | 0.007 |
RMSD bond angle | 0.899 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.18rc2_3793) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 41.080 | 1.947 |
High resolution limit [Å] | 1.880 | 1.880 |
Number of reflections | 139409 | 13587 |
<I/σ(I)> | 7.25 | |
Completeness [%] | 97.8 | |
Redundancy | 6.8 | |
CC(1/2) | 0.995 | 0.584 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG |