8BLL

Structure of RutB

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-07-14
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	P 1
Unit cell lengths	69.456, 108.609, 124.341
Unit cell angles	85.66, 83.22, 74.34

Refinement procedure

Resolution	47.000 - 1.540
R-factor	0.209
Rwork	0.207
R-free	0.24340
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.012
RMSD bond angle	1.122
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	PHENIX (1.18rc2_3793)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.000	1.590
High resolution limit [Å]	1.540	1.540
Number of reflections	472783	47452
<I/σ(I)>	7.2
Completeness [%]	87.8
Redundancy	3.3
CC(1/2)	0.974	0.390

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	PEG