8BFH
CNOT11
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-02-21 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.979 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 42.937, 27.180, 70.961 |
| Unit cell angles | 90.00, 98.39, 90.00 |
Refinement procedure
| Resolution | 29.230 - 2.200 |
| R-factor | 0.2333 |
| Rwork | 0.231 |
| R-free | 0.25020 |
| Structure solution method | SAD |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.546 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX (1.20.1_4487) |
| Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 29.230 | 2.279 |
| High resolution limit [Å] | 2.200 | 2.200 |
| Number of reflections | 7648 | 447 |
| <I/σ(I)> | 12.84 | |
| Completeness [%] | 89.5 | |
| Redundancy | 12.84 | |
| CC(1/2) | 0.997 | 0.558 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 292 | 11% (w/v) PEG 3500, 0.2M Ammonium acetate, 0.1 M MES pH 5.5 |
