8BBJ
Secretagogin (mouse) in complex with its target peptide from Syntaxin-4
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 110 |
Detector technology | PIXEL |
Collection date | 2021-02-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.96863 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.409, 103.134, 121.656 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 78.680 | 2.780 |
High resolution limit [Å] | 2.650 | 2.650 |
Rmerge | 0.070 | 0.678 |
Rpim | 0.059 | 0.574 |
Number of reflections | 28954 | 3847 |
<I/σ(I)> | 8.2 | 1.4 |
Completeness [%] | 98.2 | |
Redundancy | 3.3 | |
CC(1/2) | 0.998 | 0.598 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 8 | 277 | 0.1 M Na cacodylate pH 5.5, 0.2 M NH4SO4, 25% v/v PEGSM (PEG-smear) |