8BAD
Tpp80Aa1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-05-27 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.97628 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 133.827, 63.853, 107.292 |
Unit cell angles | 90.00, 120.40, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 57.730 | 57.760 | 1.840 |
High resolution limit [Å] | 1.810 | 4.910 | 1.810 |
Rmeas | 0.128 | 0.040 | 2.654 |
Rpim | 0.048 | 0.015 | 1.020 |
Total number of observations | 25947 | 23361 | |
Number of reflections | 71433 | 3689 | 3495 |
<I/σ(I)> | 11.8 | 56.4 | 0.6 |
Completeness [%] | 100.0 | 100 | 100 |
Redundancy | 7 | 7 | 6.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 297 | 0.02M sodium/potassium phosphate 0.1M Bis-tris propane 20% w/v PEG3350 |