8B7P
Crystal structure of an AA9 LPMO from Aspergillus nidulans, AnLPMOC
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-09-15 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 0.9762 |
| Spacegroup name | P 1 |
| Unit cell lengths | 47.900, 64.378, 76.237 |
| Unit cell angles | 86.46, 85.54, 68.21 |
Refinement procedure
| Resolution | 75.958 - 2.110 |
| Rwork | 0.213 |
| R-free | 0.27300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Starting model (for MR) | 4b5q |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.728 |
| Data reduction software | xia2 |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.960 | 2.170 |
| High resolution limit [Å] | 2.110 | 2.110 |
| Rmerge | 0.097 | 0.307 |
| Number of reflections | 39040 | 1271 |
| <I/σ(I)> | 4.9 | 1.8 |
| Completeness [%] | 80.5 | |
| Redundancy | 2 | |
| CC(1/2) | 0.986 | 0.779 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.2 M sodium thiocyanate 20% PEG 3350 |
