8B3K
Crystal structure of human Plexin-B1 (20-535) in the unbound state
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-15 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.97949 |
Spacegroup name | I 41 2 2 |
Unit cell lengths | 266.692, 266.692, 108.728 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 66.670 - 2.685 |
Rwork | 0.199 |
R-free | 0.24510 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3ol2 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 188.580 | 188.580 | 2.890 |
High resolution limit [Å] | 2.685 | 11.200 | 2.800 |
Rmerge | 0.374 | 0.063 | 4.090 |
Rmeas | 0.403 | 0.068 | 4.409 |
Rpim | 0.152 | 0.026 | 1.640 |
Number of reflections | 48266 | 862 | 4382 |
<I/σ(I)> | 5.9 | ||
Completeness [%] | 100.0 | ||
Redundancy | 13.5 | 11.6 | 14 |
CC(1/2) | 0.993 | 0.998 | 0.612 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 | 291 | 1.0 M sodium acetate, 0.2 M cadmium sulphate, 0.1 M HEPES, pH 7.5 |