8AZZ
KRAS-G12V in complex with BI-2865
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-11-22 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.999824 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 86.476, 40.709, 55.989 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.220 - 1.020 |
R-factor | 0.1461 |
Rwork | 0.145 |
R-free | 0.16690 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8afb |
RMSD bond length | 0.008 |
RMSD bond angle | 1.046 |
Data reduction software | XDS |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | PHENIX (dev_4839) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.989 | 1.128 |
High resolution limit [Å] | 1.020 | 1.025 |
Rmerge | 0.037 | 0.711 |
Number of reflections | 74206 | 3711 |
<I/σ(I)> | 24.2 | 1.9 |
Completeness [%] | 94.5 | 62.6 |
Redundancy | 12.1 | 6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 277 | 0.2mM Magnesium Chloride, 20% PEG 2000, 100mM sodium acetate pH 4.4 |