8AR6
Structure of Delta 57-NCOA7 in space group P41212
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-18 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9537 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 89.623, 89.623, 165.897 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 60.880 - 2.200 |
R-factor | 0.1936 |
Rwork | 0.191 |
R-free | 0.23840 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4acj |
RMSD bond length | 0.002 |
RMSD bond angle | 0.500 |
Data reduction software | xia2 |
Data scaling software | Aimless (1.20.1_4487) |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 60.880 | 2.279 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.077 | 0.704 |
Rpim | 0.031 | 0.294 |
Number of reflections | 34845 | 3402 |
<I/σ(I)> | 18.72 | |
Completeness [%] | 99.1 | |
Redundancy | 6.7 | |
CC(1/2) | 0.997 | 0.697 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 0.2 M di ammonium hydrogen citrate, 20% w/v PEG 3350 |