Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-04-07 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 145.253, 153.039, 62.801 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.545 - 1.853 |
Rwork | 0.190 |
R-free | 0.22900 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4mj1 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.601 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.919 |
High resolution limit [Å] | 1.853 | 1.853 |
Number of reflections | 119532 | 11509 |
<I/σ(I)> | 13.99 | |
Completeness [%] | 99.6 | |
Redundancy | 13.2 | |
CC(1/2) | 0.999 | 0.737 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293.15 | PEG 3.350 Lithium Chloride HEPES |