Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06DA |
Synchrotron site | SLS |
Beamline | X06DA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2020-09-03 |
Detector | DECTRIS PILATUS 2M-F |
Wavelength(s) | 1 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 144.488, 152.305, 62.578 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 47.898 - 1.887 |
Rwork | 0.174 |
R-free | 0.21150 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4mj1 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.620 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | REFMAC |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 1.935 |
High resolution limit [Å] | 1.887 | 1.887 |
Number of reflections | 111193 | 17862 |
<I/σ(I)> | 15.63 | |
Completeness [%] | 99.9 | |
Redundancy | 13.4 | |
CC(1/2) | 0.990 | 0.690 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293.15 | PEG 3.350 Lithium Chloride HEPES |