8ADC
Viral tegument-like DUBs
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-24 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9762 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 37.121, 70.295, 75.890 |
Unit cell angles | 90.00, 101.84, 90.00 |
Refinement procedure
Resolution | 51.060 - 1.700 |
R-factor | 0.1993 |
Rwork | 0.198 |
R-free | 0.23510 |
Structure solution method | SIR |
RMSD bond length | 0.007 |
RMSD bond angle | 0.836 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | SHELXDE |
Refinement software | PHENIX (1.20_4478) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 80.000 | 1.800 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.079 | 1.180 |
Rmeas | 0.080 | 1.410 |
Number of reflections | 81659 | 13147 |
<I/σ(I)> | 8.5 | 1 |
Completeness [%] | 98.8 | 98.3 |
Redundancy | 3.4 | 3.1 |
CC(1/2) | 0.997 | 0.535 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 298 | 0.2 M sodium chloride, 0.1 M BisTris pH 5.5, 25 % w/v PEG 3350 |