8A9W
Crystal structure of PulL C-ter domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-07-03 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.987 |
Spacegroup name | I 21 3 |
Unit cell lengths | 80.300, 80.300, 80.300 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 56.780 - 1.895 |
R-factor | 0.24464 |
Rwork | 0.241 |
R-free | 0.27651 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | NMR structure |
RMSD bond length | 0.007 |
RMSD bond angle | 1.291 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.781 | 1.927 |
High resolution limit [Å] | 1.895 | 1.895 |
Rmerge | 0.073 | 1.814 |
Rmeas | 0.074 | 1.837 |
Rpim | 0.012 | 0.291 |
Number of reflections | 7013 | 356 |
<I/σ(I)> | 30.3 | 2.8 |
Completeness [%] | 100.0 | |
Redundancy | 39.5 | |
CC(1/2) | 0.999 | 0.782 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 291 | 0.5 M LiSO4 and 15%w/v PEG 8K |