8A8X
TRIM7 PRYSPRY in complex with a MNV1-NS3 peptide HDDFGLQ
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04 |
Synchrotron site | Diamond |
Beamline | I04 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2022-04-14 |
Detector | DECTRIS EIGER2 XE 16M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 51.252, 53.668, 73.595 |
Unit cell angles | 90.00, 105.55, 90.00 |
Refinement procedure
Resolution | 28.337 - 2.370 |
Rwork | 0.189 |
R-free | 0.26370 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 8a5l |
RMSD bond length | 0.009 |
RMSD bond angle | 1.653 |
Data reduction software | xia2 (FastDP) |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.910 | 2.430 |
High resolution limit [Å] | 2.370 | 2.370 |
Number of reflections | 15418 | 712 |
<I/σ(I)> | 6.8 | |
Completeness [%] | 97.4 | |
Redundancy | 3.3 | |
CC(1/2) | 1.000 | 0.600 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 291.15 | 1 M DL-Malic Acid pH 5, 0.1 M BIS-TRIS Propane pH 6.3 |