8A4E
Room temperature structure of AtPhot2LOV2 in a photostationary equilibrium
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2022-02-02 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.9677 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 41.555, 41.555, 132.850 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.230 - 1.960 |
R-factor | 0.1889 |
Rwork | 0.187 |
R-free | 0.22470 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 6qqk |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.20_4459) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.660 | 2.080 |
High resolution limit [Å] | 1.960 | 1.960 |
Rpim | 0.082 | 0.564 |
Number of reflections | 7757 | 3612 |
<I/σ(I)> | 5.7 | 1.5 |
Completeness [%] | 91.9 | |
Redundancy | 8.4 | |
CC(1/2) | 0.980 | 0.670 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 293 | 100 mM MES pH 6.0, 4 to 9 % PEG8000, and 50 to 200 mM calcium acetate |