8A16
Human PTPRM domains FN3-4, in spacegroup P212121
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2019-02-24 |
Detector | DECTRIS PILATUS 6M-F |
Wavelength(s) | 0.9159 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 50.682, 89.638, 128.289 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 73.480 - 2.890 |
R-factor | 0.2367 |
Rwork | 0.234 |
R-free | 0.28810 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2v5y |
RMSD bond length | 0.003 |
RMSD bond angle | 0.779 |
Data reduction software | DIALS |
Data scaling software | DIALS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 128.290 | 2.940 |
High resolution limit [Å] | 2.890 | 2.890 |
Number of reflections | 13719 | 672 |
<I/σ(I)> | 7 | |
Completeness [%] | 100.0 | |
Redundancy | 12.4 | |
CC(1/2) | 0.991 | 0.432 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 200 mM ammonium nitrate and 20% (w/v) PEG 3350 |