8YXW
TRIP4 ASCH domain in complex with a 12bp dsDNA (5'-TGAGGTACCTCC-3')
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-03-30 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 61 |
Unit cell lengths | 66.597, 66.597, 199.648 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 32.830 - 2.100 |
R-factor | 0.1965 |
Rwork | 0.194 |
R-free | 0.23870 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.975 |
Data scaling software | HKL-2000 |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.140 |
High resolution limit [Å] | 2.100 | 5.700 | 2.100 |
Rmerge | 0.149 | 0.090 | 0.806 |
Rmeas | 0.154 | 0.094 | 0.837 |
Rpim | 0.039 | 0.024 | 0.224 |
Total number of observations | 456895 | ||
Number of reflections | 29191 | 1493 | 1440 |
<I/σ(I)> | 3 | ||
Completeness [%] | 100.0 | 99.5 | 100 |
Redundancy | 15.7 | 15.2 | 14.3 |
CC(1/2) | 0.997 | 0.995 | 0.895 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289.15 | 0.2 M Ammonium acetate 0.1 M BIS-TRIS pH 5.5 25% w/v Polyethylene glycol 3,350 |