8YLZ
Structure of a cis-Geranylfarnesyl Diphosphate Synthase from Streptomyces clavuligerus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL10U2 |
Synchrotron site | SSRF |
Beamline | BL10U2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-09-14 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97880 |
Spacegroup name | P 21 2 21 |
Unit cell lengths | 42.580, 61.140, 84.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.570 - 1.600 |
R-factor | 0.1969 |
Rwork | 0.195 |
R-free | 0.22640 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.917 |
Data reduction software | iMOSFLM |
Data scaling software | pointless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.940 | 1.630 |
High resolution limit [Å] | 1.600 | 1.600 |
Rmerge | 0.045 | 0.127 |
Rmeas | 0.048 | 0.135 |
Rpim | 0.015 | 0.044 |
Total number of observations | 298879 | 12444 |
Number of reflections | 27160 | 1362 |
<I/σ(I)> | 33.2 | 11.9 |
Completeness [%] | 91.3 | |
Redundancy | 11 | 9.1 |
CC(1/2) | 0.998 | 0.989 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.7 | 289.15 | 18% (w/v) Polyethylene glycol 4000, 0.1 M MES monohydrate (pH 5.7) |